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Synthesis and reactivity of [18F]-N-fluorobenzenesulfonimide.

Abstract:
A novel [18F]NF reagent and two novel radiochemical transformations have been developed: [18F]NFSi has been prepared from sodium dibenzenesulfonimide and reacted in the presence of silyl enol ethers and allylsilanes to deliver labelled fluorinated ketones and allylic fluorides respectively; the radiosynthesis of the fluorinated A ring of vitamin D3 has also been completed with success.
Publication status:
Published

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Publisher copy:
10.1039/b701177f

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Institution:
University of Oxford
Department:
Oxford, MSD, Population Health
Role:
Author
More by this author
Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Organic Chemistry
Role:
Author
Journal:
Chemical communications (Cambridge, England)
Issue:
23
Pages:
2330-2332
Publication date:
2007-06-05
DOI:
EISSN:
1364-548X
ISSN:
1359-7345
URN:
uuid:7db2a4c6-d2c6-42ef-8e7a-dfad8a35aaee
Source identifiers:
33964
Local pid:
pubs:33964

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