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Versatile in situ gas analysis apparatus for nanomaterials reactors.

Abstract:

We report a newly developed technique for the in situ real-time gas analysis of reactors commonly used for the production of nanomaterials, by showing case-study results obtained using a dedicated apparatus for measuring the gas composition in reactors operating at high temperature (<1000 °C). The in situ gas-cooled sampling probe mapped the chemistry inside the high-temperature reactor, while suppressing the thermal decomposition of the analytes. It thus allows a more accurate study of th...

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Publication status:
Published

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Publisher copy:
10.1021/ac5022858

Authors


Meysami, SS More by this author
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Institution:
University of Oxford
Department:
Oxford, MPLS, Materials
Publisher:
American Chemical Society
Journal:
Analytical chemistry
Volume:
86
Issue:
17
Pages:
8850-8856
Publication date:
2014-09-05
DOI:
EISSN:
1520-6882
ISSN:
0003-2700
URN:
uuid:7acaae05-04d5-4906-8eb7-380ea88a3701
Source identifiers:
478428
Local pid:
pubs:478428
Language:
English

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