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Single-crystal X-ray and neutron powder diffraction investigation of the phase transition in tetrachlorobenzene.

Abstract:

The polymorphic phase transition of 1,2,4,5-tetrachlorobenzene (TCB) has been investigated using neutron powder diffraction and single-crystal X-ray diffraction. The diffraction experiments show a reversible phase change that occurs as a function of temperature with no apparent loss of sample quality on transition between the two phases. Neutron powder diffraction gives detailed information on the molecular structural changes and lattice parameters from 2 K to room temperature. The structure ...

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Publication status:
Published

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Publisher copy:
10.1107/s0108768105042102

Authors


Barnett, SA More by this author
Broder, CK More by this author
Shankland, K More by this author
Ibberson, RM More by this author
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Journal:
Acta crystallographica. Section B, Structural science
Volume:
62
Issue:
Pt 2
Pages:
287-295
Publication date:
2006-04-05
DOI:
EISSN:
1600-5740
ISSN:
0108-7681
URN:
uuid:7a2c936b-ce27-405b-8f09-ba7c71664458
Source identifiers:
118910
Local pid:
pubs:118910
Language:
English

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