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Low field CIDNP of amino acids and proteins: characterization of transient radicals and NMR sensitivity enhancement

Abstract:

A new method for measuring and exploiting the magnetic field dependence of chemically induced dynamic nuclear polarization (CIDNP) is described. A solution of an amino acid or protein together with a flavin photosensitizer is irradiated with laser light at a position in the bore of a superconducting NMR magnet where the field is between 0.1 T and 7.0 T. The polarized sample is then transferred by rapid injection into an NMR tube at the centre of the magnet (at 9.4 T), where the spectrum is re...

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Publication status:
Published

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Publisher copy:
10.1080/00268970110113988

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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Physical and Theoretical Chem
Role:
Author
Volume:
100
Issue:
8
Pages:
1261-1269
Publication date:
2002-04-05
DOI:
EISSN:
1362-3028
ISSN:
0026-8976
URN:
uuid:7743a284-e891-4431-aca6-58f785c94e3c
Source identifiers:
38250
Local pid:
pubs:38250

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