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Binuclear lanthanide complexes as magnetic resonance and optical imaging probes for redox sensing

Abstract:
We report a family of lanthanide(III) complexes that act as redox probes via both magnetic resonance (MR) and luminescence outputs. The ligands are functionalized with nitro, azobenzene and azide groups which are reduced to a common aniline product, and each responds to both chemical and biocatalytic reductive conditions at different cathodic onset potentials. By judicious choice of complexed Ln(III), the probes can be optimized either for use in MR imaging (Ln = Gd), or as highly efficient turn-on luminescence probes (Ln = Tb). The Tb(III) analogues are essentially nonemissive, until reductive generation of the aniline affords a complex which when excited by visible light (488 nm) emits green light with a quantum yield of 45% and millisecond long luminescent lifetimes (ms). The tunable redox response and imaging modalities of these versatile complexes have the potential to open up new approaches to redox sensing, such as the imaging of hypoxic environments in biology.
Publication status:
Published
Peer review status:
Peer reviewed

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Publisher copy:
10.1002/chem.202404748

Authors


More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Role:
Author
More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Role:
Author
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Institution:
University of Oxford
Division:
MSD
Department:
Oncology
Role:
Author
ORCID:
0000-0001-5160-0952
More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Role:
Author
More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Role:
Author


More from this funder
Funder identifier:
https://ror.org/0439y7842
Grant:
EP/S023828/1
EP/S019901/1
Programme:
OxICFM
More from this funder
Funder identifier:
https://ror.org/054225q67
Grant:
C6078/A2873
More from this funder
Funder identifier:
https://ror.org/0472cxd90
Grant:
ERC CoG-819580
More from this funder
Funder identifier:
https://ror.org/00yjd3n13
Grant:
P500PN_214322


Publisher:
Wiley
Journal:
Chemistry - A European Journal More from this journal
Volume:
31
Issue:
30
Article number:
e202404748
Publication date:
2025-05-03
Acceptance date:
2025-04-14
DOI:
EISSN:
1521-3765
ISSN:
0947-6539


Language:
English
Keywords:
Pubs id:
2118137
Local pid:
pubs:2118137
Deposit date:
2025-04-14

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