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Measuring spin relaxation rates using satellite exchange NMR spectroscopy

Abstract:

An approach to the indirect measurement of nuclear spin relaxation rates of low-magnetogyric ratio (γ) nuclei using the process of satellite exchange is described. The method does not require the observation of, or even the ability to provide radio-frequency pulses to, the low-γ nucleus, but requires this to be scalar coupled to an NMR observable nucleus, such as 31P or 1H, making it especially attractive for the study of diamagnetic transition metals. In situations where spin relaxation is d...

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Publication status:
Accepted
Peer review status:
Peer reviewed
Version:
Accepted Manuscript

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Publisher copy:
10.1002/anie.201801322R1

Authors


More by this author
Institution:
University of Oxford
Division:
MPLS Division
Department:
Chemistry; Organic Chemistry
More by this author
Institution:
University of Oxford
Division:
MPLS Division
Department:
Chemistry; Organic Chemistry
More by this author
Institution:
University of Oxford
Division:
MPLS Division
Department:
Chemistry; Organic Chemistry
More by this author
Institution:
University of Oxford
Division:
MPLS Division
Department:
Chemistry; Organic Chemistry
ORCID:
0000-0001-5583-6460
Publisher:
Wiley-VCH Verlag Publisher's website
Journal:
Angewandte Chemie International Edition Journal website
Acceptance date:
2018-03-15
DOI:
ISSN:
1521-3773
Pubs id:
pubs:829884
URN:
uri:743739f3-0786-4e72-8abd-80a2cb76e50b
UUID:
uuid:743739f3-0786-4e72-8abd-80a2cb76e50b
Local pid:
pubs:829884

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