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New large volume hydrothermal reaction cell for studying chemical processes under supercritical hydrothermal conditions using time-resolved in situ neutron diffraction.

Abstract:

The design and testing of a new large volume Inconel pressure cell for the in situ study of supercritical hydrothermal syntheses using time-resolved neutron diffraction is introduced for the first time. The commissioning of this new cell is demonstrated by the measurement of the time-of-flight neutron diffraction pattern for TiO(2) (Anatase) in supercritical D(2)O on the POLARIS diffractometer at the United Kingdom's pulsed spallation neutron source, ISIS, Rutherford Appleton Laboratory. The ...

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Publication status:
Published

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Publisher copy:
10.1063/1.3514990

Authors


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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Inorganic Chemistry
Chowdhury, M More by this author
Fikremariam, H More by this author
Journal:
The Review of scientific instruments
Volume:
81
Issue:
12
Pages:
125107
Publication date:
2010-12-05
DOI:
EISSN:
1089-7623
ISSN:
0034-6748
URN:
uuid:70ae8330-a838-414b-8446-270379bb7d0d
Source identifiers:
120245
Local pid:
pubs:120245
Language:
English

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