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Structural characterization of sialylated glycoforms of H. influenzae by electrospray mass spectrometry: fragmentation of protonated and sodiated O-deacylated lipopolysaccharides.

Abstract:

Sialylated lipopolysaccharide (LPS) glycoforms from Haemophilus influenzae were characterized by tandem mass spectrometry using a new generation hyphenated mass spectrometer which combines a triple quadrupole and a linear ion trap (Q-Trap). The fragmentation of both protonated and sodiated molecular ions from O-deacylated LPS (LPS-OH) obtained in MS(2) experiments in the positive mode was studied. The MS(2) spectra of protonated ions provided unambiguous evidence for the presence and sequence...

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Publisher copy:
10.1002/rcm.2916

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Journal:
Rapid communications in mass spectrometry : RCM
Volume:
21
Issue:
6
Pages:
952-960
Publication date:
2007-01-01
DOI:
EISSN:
1097-0231
ISSN:
0951-4198
Source identifiers:
115594
Language:
English
Keywords:
Pubs id:
pubs:115594
UUID:
uuid:6e75543a-86dc-42e8-ba21-45e2ab8f3aaf
Local pid:
pubs:115594
Deposit date:
2012-12-19

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