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Scandium chloride, alkyl and phenyl complexes of diamido-donor ligands

Abstract:

Reactions of the lithiated diamido-pyridine and -amine ligands Li2N2TMSNpy or Li2N2NC2,TMS with ScCl3 in tetrahydrofuran (THF) afforded the five-coordinate scandium chloride derivatives [Sc(N2TMSNpy)Cl(THF)] 1 and [Sc(N2NC2,TMS)Cl(THF)] 2 where N2TMSNpy = MeC(2-C5H4N)(CH2NSiM3)2 and N2NC2,TMS = Me3SiN-(CH2CH2NSiMe3)2. The corresponding reactions of ScCl3 with the dilithium salts of the amino N-methylated two-carbon analogue N2NC2,Me (N2NC2,Me = MeN(CH2CH2NSiMe3)2) or of the amino N-silylated ...

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Publication status:
Published

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Publisher copy:
10.1039/b209382k

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Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Inorganic Chemistry
Role:
Author
Journal:
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS
Issue:
24
Pages:
4649-4657
Publication date:
2002-01-01
DOI:
EISSN:
1364-5447
ISSN:
1472-7773
Language:
English
Pubs id:
pubs:51213
UUID:
uuid:6ae003c5-2da7-463e-94d5-061962bf8b92
Local pid:
pubs:51213
Source identifiers:
51213
Deposit date:
2012-12-19

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