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Synthesis and structure of the gibbsite intercalation compounds [LiAl2(OH)(6)]X {X=Cl, Br, NO3} and [LiAl2(OH)(6)]Cl center dot H2O using synchrotron X-ray and neutron powder diffraction

Abstract:: Treatment of gibbsite {γ-Al(OH)3} with the lithium salts LiX {X = Cl, Br, NO3} in water leads to intercalation of both the cations and anions into the host structure to give [LiAl2-(OH)6]X·H2O {X = Cl, Br, NO3}. Thermogravimetric analysis indicates that these materials can be readily dehydrated to give highly hydroscopic, crystalline layered phases [LiAl2(OH)6]X {X = Cl, Br, NO3}. The structures of these dehydrated phases have been determined by synchrotron X-ray and neutron powder diffractio...
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APA Style

Besserguenev, A., Fogg, A., Francis, R., Price, S., OHare, D., Isupov, V., & Tolochko, B. (1997). Synthesis and structure of the gibbsite intercalation compounds [LiAl2(OH)(6)]X {X=Cl, Br, NO3} and [LiAl2(OH)(6)]Cl center dot H2O using synchrotron X-ray and neutron powder diffraction. CHEMISTRY OF MATERIALS, 9(1), 241–247.

MLA Style

Besserguenev, A., et al. “Synthesis and Structure of the Gibbsite Intercalation Compounds [LiAl2(OH)(6)]X {X=Cl, Br, NO3} and [LiAl2(OH)(6)]Cl Center Dot H2O Using Synchrotron X-Ray and Neutron Powder Diffraction.” CHEMISTRY OF MATERIALS, vol. 9, no. 1, 1997, pp. 241–47.

Chicago Style

Besserguenev, A, A Fogg, R Francis, S Price, D OHare, V Isupov, and B Tolochko. 1997. “Synthesis and Structure of the Gibbsite Intercalation Compounds [LiAl2(OH)(6)]X {X=Cl, Br, NO3} and [LiAl2(OH)(6)]Cl Center Dot H2O Using Synchrotron X-Ray and Neutron Powder Diffraction.” CHEMISTRY OF MATERIALS 9 (1): 241–47.
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Publisher copy:: 10.1021/cm960316z

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+ Besserguenev, A More by this author

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+ Fogg, A More by this author

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+ Francis, R More by this author

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+ Price, S More by this author

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+ OHare, D More by this author

Institution:

University of Oxford

Division:

MPLS

Department:

Chemistry

Sub department:

Inorganic Chemistry

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Bibliographic Details

Journal:: CHEMISTRY OF MATERIALS
Volume:: 9
Issue:: 1
Pages:: 241-247
Publication date:: 1997-01-01
DOI:: 10.1021/cm960316z
EISSN:: 1520-5002
ISSN:: 0897-4756

Item Description

Pubs id:: pubs:51450
UUID:: uuid:675b0876-1c81-431d-8b6e-e3343d8a636d
Local pid:: pubs:51450
Source identifiers:: 51450
Deposit date:: 2012-12-19

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Copyright date:: 1997

Licence:: Terms and Conditions of Use for Oxford University Research Archive

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