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Some experimental aspects of absolute configuration determination using single crystal X-ray diffraction

Abstract:
Students of single crystal X-ray diffraction are often give advice as to how best to collect their data when attempting absolute configuration determination. These 'rules' often have more grounding in gut-feeling than evidence. Thus, in an effort to provide advice and evidence that today's crystallographers can pass onto to tomorrow's young scientists, we present a systematic study of 1-deoxy-l-arabinitol, a straight chain sugar which crystalises well in the space group I41.
Publication status:
Published
Peer review status:
Peer reviewed

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Publisher copy:
10.1016/j.tetasy.2017.08.016

Authors


More by this author
Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Inorganic Chemistry
Role:
Author
More by this author
Institution:
University of Oxford
Division:
MPLS Division
Department:
Chemistry; Organic Chemistry
Role:
Author
More by this author
Institution:
University of Oxford
Division:
MPLS Division
Department:
Chemistry; Organic Chemistry
Role:
Author
Publisher:
Elsevier
Journal:
Tetrahedron Asymmetry More from this journal
Volume:
28
Issue:
10
Pages:
1330-1336
Publication date:
2017-10-12
Acceptance date:
2017-08-16
DOI:
EISSN:
1362-511X
ISSN:
0957-4166
Keywords:
Pubs id:
pubs:738071
UUID:
uuid:65a96aa1-ad30-4362-b173-e81dd611bda4
Local pid:
pubs:738071
Source identifiers:
738071
Deposit date:
2017-10-30

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