- Abstract:
-
High-resolution X-ray diffraction data were collected at T = 19 K from two similar spherical crystals of the fungal metabolite citrinin, C(13)H(14)O(5). The two data sets were of markedly different quality, one data set (MQ, medium quality) comprising a single octant of the reciprocal lattice and including reflections with obviously peculiar intensity profiles while the second (HQ, high quality) comprised a hemisphere of reflections and showed no flawed profiles. Parallel multipolar refinemen...
Expand abstract - Publication status:
- Published
- Publisher copy:
- 10.1107/s0108767304014813
-
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- Journal:
- Acta crystallographica. Section A, Foundations of crystallography
- Volume:
- 60
- Issue:
- Pt 5
- Pages:
- 365-370
- Publication date:
- 2004-09-05
- DOI:
- EISSN:
-
1600-5724
- ISSN:
-
0108-7673
- URN:
-
uuid:5386259c-dbdb-4c08-812b-f0ac882e7c18
- Source identifiers:
-
23949
- Local pid:
- pubs:23949
- Language:
- English
- Keywords:
- Copyright date:
- 2004
Journal article
On the role of data quality in experimental charge-density studies.
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