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Evidence for nucleation-growth, redistribution, and dissolution mechanisms during the course of redox cycling experiments on the C-60/NBu4C60 solid-state redox system: Voltammetric, SEM, and in situ AFM studies

Abstract:

The electrochemical reduction of solid C60 abrasively attached in the form of microcrystals to graphite and glassy carbon electrode surfaces and then immersed in acetonitrile containing 0.1 M NBu4PF6 or NBu4ClO4 as the electrolyte has been studied. Voltammetric responses observed after the initial stages of redox cycling experiments, when redistribution processes occur, are consistent with those observed previously for so-called "film" deposits. The characteristic "steady-state" shape of the ...

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Publication status:
Published

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Publisher copy:
10.1021/jp990926x

Authors


Suarez, MF More by this author
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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Physical and Theoretical Chem
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Journal:
JOURNAL OF PHYSICAL CHEMISTRY B
Volume:
103
Issue:
27
Pages:
5637-5644
Publication date:
1999-07-08
DOI:
EISSN:
1520-5207
ISSN:
1089-5647
URN:
uuid:48a0820e-065f-4693-b58a-08a33cdf8c28
Source identifiers:
37052
Local pid:
pubs:37052
Language:
English

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