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ASYMMETRIC-SYNTHESIS OF (2S,3R)-3-AMINO-2-HYDROXYDECANOIC ACID - THE UNKNOWN AMINO-ACID COMPONENT OF MICROGININ

Abstract:

3-Amino-2-hydroxydecanoic acid (AHDA) is an unusual amino acid purported to occur in the recently isolated angiotensin-converting enzyme inhibitor microgipin. In order to elucidate the stereochemistry of the naturally occurring material, and thus complete the structural assignment of microginin, both the (2R,3R)-anti-diastereoisomer and the (2S,3R)syn-diastereoisomer of AHDA have been prepared. Comparison of the 1H and 13C nmr spectroscopic data of the synthetic amino acids with that reported...

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Publication status:
Published

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Journal:
TETRAHEDRON-ASYMMETRY
Volume:
5
Issue:
2
Pages:
203-206
Publication date:
1994-02-05
DOI:
EISSN:
1362-511X
ISSN:
0957-4166
URN:
uuid:4024c3a8-b6ee-4603-a959-26e8756d6ffc
Source identifiers:
110874
Local pid:
pubs:110874
Language:
English

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