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Recent results from the in situ study of hydrothermal crystallisations using time-resolved X-ray and neutron diffraction methods.

Abstract:

We present new time-resolved powder diffraction data measured in situ during the hydrothermal crystallisation of two families of crystalline inorganic materials. In the first study, we have used time-resolved energy-dispersive X-ray diffraction (EDXRD) to follow the formation of zeolitic zinc phosphates from amine phosphates and zinc oxide in acidic solutions at 60-150 degrees C. The advantage of this method is the ability to penetrate a laboratory-sized reaction vessel and to measure data in...

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Publication status:
Published

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Publisher copy:
10.1039/b200990k

Authors


Walton, RI More by this author
Norquist, A More by this author
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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Inorganic Chemistry
Journal:
Faraday discussions
Volume:
122
Pages:
331-341
Publication date:
2003
DOI:
EISSN:
1364-5498
ISSN:
1359-6640
URN:
uuid:3e4ce71d-1c76-403b-93d6-776de38037b2
Source identifiers:
51220
Local pid:
pubs:51220
Language:
English

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