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Thermo-mechanical properties of mixed-matrix membranes encompassing zeolitic imidazolate framework-90 and polyvinylidine difluoride: ZIF-90/PVDF nanocomposites

Abstract:
Mixed-matrix membranes are contemporary nanocomposite materials with many potential applications, from liquid and gas separations to chemical sensors and biomedicine. We report fabrication of a metal-organic framework (MOF)-based nanocomposite, combining polyvinylidene difluoride (PVDF) polymer as the matrix and ZIF-90 nanocrystals of up to 30 wt. % filler content. The focus is to establish the processing - microstructure - mechanical property relationships. We reveal the importance for quantifying salient effects of the filler contents: (i) tensile strength degrades beyond 10 wt. % and (ii) mechanical toughness declines due to membrane embrittlement. These are vital mechanical aspects but widely overlooked in the emergent field of MOF membranes and composites.
Publication status:
Published
Peer review status:
Peer reviewed

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Publisher copy:
10.1063/1.4986565

Authors


More by this author
Institution:
University of Oxford
Division:
MPLS Division
Department:
Engineering Science
Role:
Author
More by this author
Institution:
University of Oxford
Division:
MPLS Division
Department:
Engineering Science
Oxford college:
Balliol College
Role:
Author


Publisher:
American Institute of Physics
Journal:
APL Materials More from this journal
Volume:
5
Issue:
8
Pages:
086104
Publication date:
2017-08-01
Acceptance date:
2017-08-06
DOI:
EISSN:
2166-532X


Keywords:
Pubs id:
pubs:724782
UUID:
uuid:3762c53b-e809-4669-bbb8-aa932b6b2fa9
Local pid:
pubs:724782
Source identifiers:
724782
Deposit date:
2017-11-11

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