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The Oxford-Diamond In Situ Cell for studying chemical reactions using time-resolved X-ray diffraction.

Abstract:

A versatile, infrared-heated, chemical reaction cell has been assembled and commissioned for the in situ study of a range of chemical syntheses using time-resolved energy-dispersive X-ray diffraction (EDXRD) on Beamline I12 at the Diamond Light Source. Specialized reactor configurations have been constructed to enable in situ EDXRD investigation of samples under non-ambient conditions. Chemical reactions can be studied using a range of sample vessels such as alumina crucibles, steel hydrother...

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Publication status:
Published

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Publisher copy:
10.1063/1.4746382

Authors


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Institution:
University of Oxford
Department:
Oxford, MPLS, Chemistry, Inorganic Chemistry
Role:
Author
Journal:
The Review of scientific instruments
Volume:
83
Issue:
8
Pages:
084101
Publication date:
2012-08-05
DOI:
EISSN:
1089-7623
ISSN:
0034-6748
URN:
uuid:2e927239-32dc-4ec0-80a8-a8c3cd67dfb9
Source identifiers:
356448
Local pid:
pubs:356448
Language:
English

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