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Quantitative EFTEM measurement of the composition of embedded particles

Abstract:

The optimisation of parameters is investigated for the compositional analysis of nanometre-sized particles embedded in a matrix by energy-filtered transmission electron microscopy. The specific example of Cu-rich particles in a Fe matrix is used both to model and to explore the experimental limits of detection and characterisation. Modelling of alternative procedures for background extrapolation as a function of the number of pre-edge windows confirmed that greater accuracy in a fixed analysi...

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Publication status:
Published

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Publisher copy:
10.1007/s10853-006-0093-9

Authors


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Institution:
University of Oxford
Department:
Oxford, MPLS, Materials
Titchmarsh, JM More by this author
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Institution:
University of Oxford
Department:
Oxford, MPLS, Materials
Volume:
41
Issue:
14
Pages:
4394-4404
Publication date:
2006-07-05
DOI:
EISSN:
1573-4803
ISSN:
0022-2461
URN:
uuid:2da585f8-65f9-4944-8479-2db5f6b812b1
Source identifiers:
14905
Local pid:
pubs:14905

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