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Structural investigations of a lead(IV) tetraacetate-pyridine complex.

Abstract:

A 1 : 1 crystalline complex of lead(IV) tetraacetate and pyridine (LTA-py) has been prepared. The single-crystal X-ray structure, at 296 and 150 K, establishes the presence of a relatively short Pb-N bond (2.307 A) within an intriguing seven-coordinate lead inner sphere consisting of the pyridine ligand and two bidentate and two monodentate acetate ligands. The pyridine occupies a surprising amount of the available coordination space and has induced a dramatic change in coordination compared ...

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Publication status:
Published

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Publisher copy:
10.1039/b506366c

Authors


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Institution:
University of Oxford
Division:
MPLS
Department:
Chemistry
Sub department:
Organic Chemistry
Role:
Author
Journal:
Dalton transactions (Cambridge, England : 2003) More from this journal
Issue:
19
Pages:
3195-3203
Publication date:
2005-10-01
DOI:
EISSN:
1477-9234
ISSN:
1477-9226
Language:
English
Pubs id:
pubs:33236
UUID:
uuid:21b04169-4872-42a2-8151-5cb478aea16a
Local pid:
pubs:33236
Source identifiers:
33236
Deposit date:
2012-12-19

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