- Abstract:
-
Solution-state NMR spectroscopy remains the primary method for characterizing synthetic supramolecular assemblies. Yet, in their NMR spectra, relaxation interference effects can significantly alter peak intensities hindering interpretation. Here, we present a simple experiment for synthetic chemists to analyse this effect, allowing interpretion of these distorted spectra and validation of spectral assignments. We apply this experiment to synthetic porphyrin oligomers with molecular weights ap...
Expand abstract - Publication status:
- Published
- Peer review status:
- Peer reviewed
- Version:
- Accepted manuscript
- Files:
-
-
(pdf, 2.3MB)
-
- Publisher copy:
- 10.1039/c6cc02544g
-
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- Funding agency for:
- Baldwin, A
- Publisher:
- Royal Society of Chemistry Publisher's website
- Journal:
- Chemical Communications Journal website
- Volume:
- 52
- Issue:
- 47
- Pages:
- 7450-7453
- Publication date:
- 2016-04-05
- Acceptance date:
- 2016-04-15
- DOI:
- ISSN:
-
1364-548X and 1359-7345
- Pubs id:
-
pubs:617739
- URN:
-
uri:1dd7e872-ff50-4e27-bd90-b3bf62600ad9
- UUID:
-
uuid:1dd7e872-ff50-4e27-bd90-b3bf62600ad9
- Local pid:
- pubs:617739
- Language:
- English
- Keywords:
- Copyright holder:
- Royal Society of Chemistry
- Copyright date:
- 2016
- Notes:
- © Royal Society of Chemistry 2016
Journal article
Harnessing NMR relaxation interference effects to characterise supramolecular assemblies.
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+ Biotechnology and Biological Sciences Research Council
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