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2H[19F] REDOR for distance measurements in biological solids using a double resonance spectrometer.

Abstract:

A new approach for distance measurements in biological solids employing 2H[19F] rotational echo double resonance was developed and validated on 2H,19F-D-alanine and an imidazopyridine based inhibitor of the gastric H+/K+-ATPase. The 2H-19F double resonance experiments presented here were performed without 1H decoupling using a double resonance NMR spectrometer. In this way, it was possible to benefit from the relatively longer distance range of fluorine without the need of specialized fluorin...

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Publication status:
Published

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Publisher copy:
10.1016/j.jmr.2003.10.005

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Institution:
University of Oxford
Department:
Oxford, MSD, Biochemistry
Journal:
Journal of magnetic resonance (San Diego, Calif. : 1997)
Volume:
166
Issue:
1
Pages:
1-10
Publication date:
2004-01-05
DOI:
EISSN:
1096-0856
ISSN:
1090-7807
URN:
uuid:1d92d2a3-f54c-464e-90c9-876c551505f6
Source identifiers:
99823
Local pid:
pubs:99823

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